2,4-二甲基-2-戊醇合成路线 （共 41 条）
反应条件
nitrous acid methyl ester; nitrogen(II) oxide T=296°C; Decomposition; oxidation; P=740 Torr; Photolysisgas phase; Kinetics;
参考文献
Atkinson; Aschmann
Environmental Science and Technology, 1995 , vol. 29, # 2 p. 528 - 536
反应条件
potassium permanganate in water
参考文献
Murray, Robert W.; Gu, Hong
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 11 p. 751 - 758
参考文献
de Graef
Bulletin des Societes Chimiques Belges, 1931 , vol. 40, p. 326
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Wibaut et al.
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 347
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 266,267
反应条件
nitrous acid methyl ester; nitrogen(II) oxide T=296°C; Decomposition; oxidation; P=740 Torr; Photolysisgas phase; Kinetics;
参考文献
Atkinson; Aschmann
Environmental Science and Technology, 1995 , vol. 29, # 2 p. 528 - 536
参考文献
Pawlow
Justus Liebigs Annalen der Chemie, 1874 , vol. 173, p. 194
反应条件
potassium hydride
1.)THF, 2 h, reflux, 2.) 0.5 h at 20 deg C, reflux, 1 h; Multistep reaction;
参考文献
Begtrup, Mikael
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1609 - 1618
反应条件
1: With trifluorormethanesulfonic acid
T=50°C; diacetylation; 1 h;
2: With ammonium hydroxide
Title compound not separated from byproducts;
参考文献
Roussel, Christian; Rajoharison, Harivelo G.; Metzger, Jacques
Revue Roumaine de Chimie, 1991 , vol. 36, # 4-7 p. 613 - 618
反应条件
ammonium hydroxide; trifluorormethanesulfonic acid
2.) 45 min.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Rajoharison, Harivelo G.; Roussel, Christian
Bulletin de la Societe Chimique de France, 1986 , # 2 p. 307 - 313
反应条件
(i) K, benzene, (ii) /BRN= 473192/; Multistep reaction;
参考文献
Duismann,W. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1820 - 1833
反应条件
sodium cyanide in benzene
参考文献
Breslow,D.S. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 4268 - 4275
