CH3I in dichloromethane byproducts: I2; under N2, excess CH3I added to soln. of Nb complex in CH2Cl2, mixt. stirred at room temp. for 15 h during yellow product sepd.; solid filtered off, washed with CH2Cl2, dried in vac., elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 243, # 4 p. 427 - 436
methyl iodide in acetone 3 h; Ambient temperature;
参考文献
Beddoes, Roy L.; Mills, Owen S.; Stansfield, Frank
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 619 - 622