1: 3-(methylthio)thiophene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.25 h;
2: With methanol in tetrahydrofuran; hexane
T=-78°C; 0.166667 h;
3: methyl chloroformate in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
Fattuoni, Claudia; Usai, Michele; Cadoni, Enzo; Cabiddu, M. Grazia; De Montis, Stefania; Cabiddu, Salvatore
Synthesis, 2008 , # 6 p. 985 - 989