2-甲基-1,3-恶唑-4-甲酰氯合成路线 （共 3 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane
T=0 - 20°C; 3 h;
参考文献
Benoit, Georges-Emmanuel; Carey, John S.; Chapman, Alan M.; Chima, Ranjit; Hussain, Nigel; Popkin, Matthew E.; Roux, Guillaume; Tavassoli, Bahareh; Vaxelaire, Carine; Webb, Michael R.; Whatrup, David
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 88 - 95
反应条件
1: 66 percent / aq. KOH / 1 h / Heating
2: SOCl2 / 4 h / Heating
View Scheme
参考文献
Chattopadhyay, Shital K.; Kempson, James; McNeil, Alan; Pattenden, Gerald; Reader, Michael; Rippon, David E.; Waite, David
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2415 - 2428
反应条件
1: 41 percent / nickel peroxide / hexane / 2 h / Heating
2: 66 percent / aq. KOH / 1 h / Heating
3: SOCl2 / 4 h / Heating
View Scheme
参考文献
Chattopadhyay, Shital K.; Kempson, James; McNeil, Alan; Pattenden, Gerald; Reader, Michael; Rippon, David E.; Waite, David
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2415 - 2428
