1,2-二(五甲基二硅氧基)乙烷合成路线 （共 6 条）
反应条件
1: 1,2-bis-(chlorodimethylsilyl)ethane With water in toluene
T=90°C; 6 h;
2: bis-trimethylsilyl ether With trifluorormethanesulfonic acid in toluene
T=50°C;
参考文献
DOW CORNING TORAY CO., LTD.; HAYASHI, Akito; IIMURA, Tomohiro; FURUKAWA, Haruhiko; KONDO, Hidetoshi
Patent: WO2011/68250 A1, 2011 ;
Location in patent: Page/Page column 40-41 ;
反应条件
1: bis-trimethylsilyl ether With acetic acid; trifluorormethanesulfonic acid
T=45°C;
2: bis(dimethylmethoxysilyl)ethane
参考文献
DOW CORNING TORAY CO., LTD.; HAYASHI, Akito; IIMURA, Tomohiro; FURUKAWA, Haruhiko; KONDO, Hidetoshi
Patent: WO2011/68250 A1, 2011 ;
Location in patent: Page/Page column 41 ;
反应条件
(Me)3SiC3H6OC6H4CN*PtCl2
T=80°C; 2 h;
参考文献
Amako, Masaaki; Schinkel, Jonathan; Freiburger, Lee; Brook, Michael A.
Dalton Transactions, 2005 , # 1 p. 74 - 81
反应条件
platinum on activated charcoal in tetrahydrofuran
参考文献
Schuchmann,H.-P. et al.
Journal of Organometallic Chemistry, 1978 , vol. 148, p. 213 - 223
反应条件
1: 17 g / Lewatit SPC 118 / 5 h / Ambient temperature
2: Pt / 0.33 h / 50 °C
View Scheme
参考文献
Brand, Dagmar; Moretto, Hans-Heinrich; Schulze, Manfred; Wrobel, Dieter
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 3 p. 218 - 224
反应条件
Wilkinson's catalyst
参考文献
Souchek,I. et al.
Doklady Chemistry, 1975 , vol. 222, p. 305 - 307
Dokl. Akad. Nauk SSSR Ser. Khim., 1975 , vol. 222, p. 128 - 131
