(R)-(+)-3-甲基己二酸合成路线 (共 15 条)
反应条件
ruthenium trichloride; sodium periodate in tetrachloromethane; acetonitrile 5 h;
参考文献
Santos Pisoni, Diego dos; Sobieski da Costa, Jesse; Gamba, Douglas; Petzhold, Cesar Liberato; Cesar de Amorim Borges, Antonio; Ceschi, Marco Antonio; Lunardi, Paula; Saraiva Goncalves, Carlos Alberto
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 2 p. 526 - 535
反应条件
Jone's reagent in acetone T=20°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 41 p. 17023 - 17026,4
反应条件
diethyl ether Erhitzen des Reaktionsprodukts mit NH3 und AgNO3 in wss. Dioxan, zuletzt unter Zusatz von KOH;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2568
反应条件
1: 3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate); C49H76N4O4 / ethyl acetate / 18 h / -20 °C 2: potassium hydroxide; methanol / 24 h / 20 °C 3: Jone's reagent / acetone / 24 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 41 p. 17023 - 17026
反应条件
hydrogenchloride T=110°C;
参考文献
Chemische Berichte, , vol. 59, p. 1095,1096
参考文献
Journal of Organic Chemistry, , vol. 20, p. 1311,1314
反应条件
jones' reagent; ozone 1.) acetone, -78 deg C, 5 min, 2.) acetone, 0 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Asymmetry, , vol. 9, # 9 p. 1605 - 1614
反应条件
Catalyst M-Chromium oxide; sulfuric acid
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>107, p. 207
反应条件
water; silver(l) oxide
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 41, p. 690
反应条件
(i) O3, (ii) AcOOH, AcOH; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 721, p. 133 - 153