6-溴-2-苯并噻唑啉酮合成路线 （共 14 条）
反应条件
bromine in chloroform T=27°C; 3 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 1503 - 1509
反应条件
K2S; copper(ll) bromide T=120°C; 15 h;
参考文献
RSC Advances, , vol. 4, # 12 p. 6090 - 6093
参考文献
Journal of Organic Chemistry, , vol. 18, p. 1092,1099
参考文献
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, , vol. 5, p. 11,14, 16, 18
参考文献
Journal of the Chemical Society, , p. 125,145
反应条件
1: aqueous HCl View Scheme
参考文献
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, , vol. 5, p. 11,14, 16, 18
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate in N,N-dimethyl-formamide T=20 - 25°C; 0.5 h;
参考文献
Petrova; Petrov; Antonova; Kalcheva
Synthetic Communications, 2003 , vol. 33, # 24 p. 4355 - 4366
反应条件
sodium hydroxide; water T=100°C; 15 h;
参考文献
Cowart, Marlon D.; Ku, Yi-Yin; Chang, Sou-Jen; Fernando, Dilinie P.; Grieme, Timothy A.; Altenbach, Robert J.
Patent: US2004/248899 A1, 2004 ;
Location in patent: Page 22 ;
反应条件
1: With trichlorophosphate in N,N-dimethyl-formamide T=100°C; 2: With potassium carbonate in water; N,N-dimethyl-formamide T=20 - 35°C; pH=> 10; 1 h;
参考文献
CRITICAL THERAPEUTICS, INC.
Patent: WO2007/146066 A2, 2007 ;
Location in patent: Page/Page column 88-89 ;
反应条件
1: With sodium hydroxide; water T=20 - 100°C; 2: With acetic acid in water T=0°C; pH=6;
参考文献
Cowart, Marlon D.; Ku, Yi-Yin; Chang, Sou-Jen; Fernando, Dilinie P.; Grieme, Timothy A.; Altenbach, Robert J.
Patent: US2004/224953 A1, 2004 ;
