(S)-3-丁烯-1,2-二醇合成路线 （共 20 条）
反应条件
chiral oligo-(salen)Co(OTs) complexes; lutidinium p-toluene sulfonate; water in dichloromethane; acetonitrile T=20°C; 4 h;
参考文献
Ready; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 11 p. 2687 - 2688
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran T=0 - 20°C; 72 h;
参考文献
Ready; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 11 p. 2687 - 2688
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran T=4°C; 12 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran T=0 - 20°C; 72 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
triethyl borane; S,S-DACHN; sodium hydrogencarbonate; 4-(N,N-dimethlyamino)pyridine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in dichloromethane Hydrolysis;
参考文献
Journal of the American Chemical Society, , vol. 121, # 37 p. 8649 - 8650
反应条件
hydrogenchloride in ethanol
参考文献
Canadian Journal of Chemistry, , vol. 54, p. 3364 - 3376
反应条件
(AcO)[(S)-substituted salen]Co(III) in water T=0°C; 12 h; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 37 p. 7010 - 7014
反应条件
water; potassium carbonate in methanol Hydrolysis; 1 h;
参考文献
Marguet, Frank; Cavalier, Jean-Francois; Verger, Robert; Buono, Gerard
European Journal of Organic Chemistry, 1999 , # 7 p. 1671 - 1678
反应条件
potassium hydroxide T=60°C; 2 h;
参考文献
Boaz, Neil W.; Falling, Stephen N.; Moore, Mary K.
Synlett, 2005 , # 10 art. no. S03205ST, p. 1615 - 1617
参考文献
Brunet, Vincent A.; Slawin, Alexandra M. Z.; O'Hagan, David
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. 61
