二甲基3,3'-(1,3-亚苯基)二丙酸酯合成路线 （共 9 条）
反应条件
1: (i) Py, (ii) (decarboxylation)
2: H2, aq. NaOH / Pd-C
3: (i) SOCl2, (ii) /BRN= 1098229/
View Scheme
参考文献
Schimelpfenig,C.W.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1493 - 1494
反应条件
1: H2, aq. NaOH / Pd-C
2: (i) SOCl2, (ii) /BRN= 1098229/
View Scheme
参考文献
Schimelpfenig,C.W.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1493 - 1494
反应条件
palladium on activated charcoal
T=300°C;
参考文献
Buchta,E.; Billenstein,S.
Justus Liebigs Annalen der Chemie, 1966 , vol. 692, p. 42 - 52
反应条件
ethanol; nickel; ethyl acetate
Hydrogenation.weiteres Reagens: Wasser;
参考文献
Ruggli; Staub
Helvetica Chimica Acta, 1936 , vol. 19, p. 439,445
参考文献
Effenberger,F.; Kurtz,W.
Chemische Berichte, 1973 , vol. 106, p. 511 - 524
参考文献
Kipping
Journal of the Chemical Society, 1888 , vol. 53, p. 41
Chemische Berichte, 1888 , vol. 21, p. 42
反应条件
1: (i) KOH, MeOH, (ii) (decarboxylation), (iii) /BRN= 102415/
2: Pd-C / 300 °C
View Scheme
参考文献
Buchta,E.; Billenstein,S.
Justus Liebigs Annalen der Chemie, 1966 , vol. 692, p. 42 - 52
反应条件
1: LiAlH4 / diethyl ether
2: NaBr, aq. H2SO4
4: (hydrolysis)
View Scheme
参考文献
Schimelpfenig,C.W.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1493 - 1494
反应条件
potassium hydroxide in methanol
参考文献
Buchta,E.; Billenstein,S.
Justus Liebigs Annalen der Chemie, 1966 , vol. 692, p. 42 - 52
