Kirmse; Horner
Justus Liebigs Annalen der Chemie, 1958 , vol. 614, p. 1
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Moulin
Helvetica Chimica Acta, 1952 , vol. 35, p. 167,175
1: 62 percent / 6 h / 130 °C
2: 90 percent / KOH / ethanol
3: oxalyl chloride, pyridine / benzene / 0.5 h / 15 °C
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参考文献
Klaubert, Dieter H.; Sellstedt, John H.; Guinosso, Charles J.; Bell, Stanley C.; Capetola, Robert J.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 6 p. 748 - 752
1: benzyl azide With triphenylphosphine on polystyrene in tetrahydrofuran
T=20°C; Staudinger reaction; 4 h;
2: 4-bromomethyl-benzonitrile in tetrahydrofuran
T=20°C; 16 h;
3: With potassium hydroxide in methanol
T=65°C; 4 h; Further stages.;
1: 85 percent / benzene / 5 h / Ambient temperature
2: xylene / 0.08 h / Heating
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参考文献
Husinec, Suren; Porter, Alexander E. A.; Roberts, James S.; Strachan, Calum H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2517 - 2522
