N-(4-碘苯基)乙酰胺合成路线 （共 72 条）
反应条件
In(OSO2CF3)3; iodine cloride in dichloromethane; acetonitrile T=20°C; 0.5 h;
参考文献
Johnsson, Richard; Meijer, Andreas; Ellervik, Ulf
Tetrahedron, 2005 , vol. 61, # 49 p. 11657 - 11663
反应条件
pyridine; acetic anhydride in ethyl acetate
参考文献
Nagano, Tetsuo; Urano, Yasuteru; Setsukinai, Ken-ichi
Patent: US2003/153027 A1, 2003 ;
反应条件
pyridine in tetrahydrofuran Heating;
参考文献
Hrobarik, Peter; Hrobarikova, Veronika; Sigmundova, Ivica; Zahradnik, Pavol; Fakis, Mihalis; Polyzos, Ioannis; Persephonis, Peter
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8726 - 8736
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 3 h;
参考文献
SANTEN PHARMACEUTICAL CO., LTD.
Patent: WO2006/22442 A1, 2006 ;
Location in patent: Page/Page column 64-65 ;
反应条件
trimethylsilylazide; iron(III) chloride in 1,2-dichloro-ethane T=20°C; azido-Schmidt reaction; 0.583333 h;
参考文献
Yadav; Reddy, B.V. Subba; Reddy, U.V. Subba; Praneeth
Tetrahedron Letters, 2008 , vol. 49, # 32 p. 4742 - 4745
反应条件
tributylphosphine; sodium iodide; niobium bromide in 1-methyl-pyrrolidin-2-one T=180°C; Finkelstein reaction; 16 h; Inert atmosphereMolecular sieveSealed tube;
参考文献
Cant, Alastair A.; Bhalla, Rajiv; Pimlott, Sally L.; Sutherland, Andrew
Chemical Communications, 2012 , vol. 48, # 33 p. 3993 - 3995
反应条件
dihydrogen peroxide in water T=25°C; 8 h; Green chemistry;
参考文献
Sun, Xi; Wang, Min; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Green Chemistry, 2013 , vol. 15, # 12 p. 3289 - 3294
反应条件
triethylamine in dichloromethane
参考文献
EP610032 A1, ;
EP 0610032 A1
反应条件
1: With hydroxymethylpolystyrene resin-CH2OCO2-N-imidazol in 1,2-dichloro-ethane T=60°C; 72 h; 2: With trifluoroacetic acid in dichloromethane T=35°C; Beckmann rearrangement; 16 h;
参考文献
Tetrahedron Letters, , vol. 44, # 47 p. 8581 - 8584
反应条件
1: ferrosulfate; ammonia View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 17, p. 487
