1,3-二羟基丙酮二聚体合成路线 (共 44 条)
反应条件
C32H30N4O4Pd2(2+); p-benozquinone in water; acetonitrile T=23°C; 4 h;
参考文献
Painter, Ron M.; Pearson, David M.; Waymouth, Robert M.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 49 p. 9456 - 9459
反应条件
triethylamine; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride in N,N-dimethyl-formamide T=100°C; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 116, p. 197 - 208
反应条件
triethylamine; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride in N,N-dimethyl-formamide T=100°C; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 116, p. 197 - 208
反应条件
triethylamine; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride in N,N-dimethyl-formamide T=100°C; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 116, p. 197 - 208
反应条件
triethylamine; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride in N,N-dimethyl-formamide T=60°C; 1 h; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 116, p. 197 - 208
反应条件
triethylamine; thiazolium salt in N,N-dimethyl-formamide T=100°C; influence of amount of paraformaldehyde, paraformaldehyde:catalyst ratio, reaction temperature and time, other amine bases; MechanismProduct distribution;
参考文献
Carbohydrate Research, , vol. 116, p. 197 - 208
反应条件
ammonium chloride in ammonium hydroxide T=80°C; 0.5 h;
参考文献
Journal of Medicinal Chemistry, , vol. 50, # 17 p. 4147 - 4161
反应条件
N-methylamine hydrochloride
参考文献
LG Life Sciences, Ltd.
Patent: US6511978 B1, 2003 ;
US 6511978 B1
反应条件
1: With acetic acid in butan-1-ol T=20°C; 72 h; 2: With nitric acid; sodium nitrite T=20°C; 6 h; Further stages.;
参考文献
De Figueiredo, Renata Marcia; Coudray, Laetitia; Dubois, Joelle
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 20 p. 3299 - 3309
反应条件
bei mehrjaehrigem Aufbewahren eines Handelspraeparats unter Ausschluss von Licht und Luft; Prod.5: Milchsaeure;
参考文献
Sanna
Rend.Fac.Sci.Cagliari, 1946 , vol. 16, p. 249