1,2-丙烷二醇 2-乙酸酯合成路线 (共 11 条)
反应条件
water; Amberlite IR 120 resin T=80°C; 3 h; Product distribution / selectivity;
参考文献
Council of Scientific and Industrial Research
Patent: US2005/222452 A1, 2005 ;
Location in patent: Page/Page column 10-11 ;
反应条件
hydrogenchloride; water T=50°C; 0.5 h; Conversion of starting material;
参考文献
Council of Scientific and Industrial Research
Patent: US2005/222452 A1, 2005 ;
Location in patent: Page/Page column 12 ;
反应条件
water; Amberlite IR 120 resin T=80°C; 3 h; Product distribution / selectivity;
参考文献
Council of Scientific and Industrial Research
Patent: US2005/222452 A1, 2005 ;
Location in patent: Page/Page column 10-11 ;
反应条件
hydrogenchloride; water T=50°C; 0.5 h; Conversion of starting material;
参考文献
Council of Scientific and Industrial Research
Patent: US2005/222452 A1, 2005 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; Ru/Al2O3 in water
T=50 - 150°C; P=51716.2 Torr; 2 - 3 h; Conversion of starting material;
参考文献
Council of Scientific and Industrial Research
Patent: US2005/222452 A1, 2005 ;
Location in patent: Page/Page column 10; 12 ;
反应条件
tetra-n-butylammonium acetate in acetonitrile
T=40°C; regioselective reaction;
参考文献
Zhou, Yixuan; Rahm, Martin; Wu, Bin; Zhang, Xiaoling; Ren, Bo; Dong, Hai
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11618 - 11622
反应条件
ethanol; nickel
P=33097.9 Torr; Hydrogenation;
参考文献
Pujo et al.
Bulletin de la Societe Chimique de France, 1955 , p. 974,977, 980
反应条件
pyridine
T=37°C; 10 h; pronase E (proteases from Streptomyces griseus); Title compound not separated from byproducts;
参考文献
Bhattacharya, A; Ali, E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 12 p. 898 - 899
反应条件
bis(acetonitrile)chloronitropalladium(II)
T=25°C; 2 h; various catalysts, times, O2 atmosphere with 18O containing complex; further products; Product distribution;
参考文献
Mares, Frank; Diamond, Steven E.; Regina, Francis J.; Solar, Jeffrey P.
Journal of the American Chemical Society, 1985 , vol. 107, # 12 p. 3545 - 3552
反应条件
dihydrogen peroxide in water
other 4-substituted and unsubstituted 1,3-dioxacyclanes; var. temp and time; catalyze FeCl3; Product distributionMechanism;
参考文献
Nazarov, M. N.; Kuramshin, E. M.; Zlotskii, S. S.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 7.1 p. 1258 - 1260
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 7 p. 1458 - 1460