1,3,5-三甲氧基苯合成路线 (共 273 条)
反应条件
sodium; copper monoiodide in N-methyl-acetamide; methanol
反应条件
potassium carbonate in acetone
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1549 - 1550
反应条件
palladium (II) trifluoroacetate; trifluoroacetic acid in dimethyl sulfoxide; N,N-dimethyl-formamide T=70°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 10 p. 4744 - 4761
反应条件
bis-triphenylphosphine-palladium(II) chloride; water; sodium hydroxide in tetrahydrofuran T=70°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 67, # 11 p. 2125 - 2131
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium hydroxide in water; toluene T=120°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6726 - 6730
Angewandte Chemie, , vol. 121, # 36 p. 6854 - 6858
反应条件
chloro-trimethyl-silane; water; potassium iodide in acetonitrile T=20°C; 0.1 h;
参考文献
Tetrahedron Letters, , vol. 36, # 28 p. 5093 - 5094
反应条件
Cu2Cl2 in N,N-dimethyl-formamide T=130°C; 6 h;
参考文献
Organic Preparations and Procedures International, , vol. 35, # 2 p. 225 - 227
反应条件
(4R,5R)-DIOP; [Rh(OH)(cycloocta-1,5-diene)]2; water; sodium hydroxide in toluene T=120°C; Heck-Mizoroki olefination; 30 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 5 p. 992 - 995
反应条件
sodium tetrahydroborate; sodium ditelluride; acetic acid in ethanol 4 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
tris-(dibenzylideneacetone)dipalladium(0); di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in N,N-dimethyl-formamide T=100°C; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 1 p. 125 - 129