双(4-二甲基氨基苯基 )乙炔合成路线 （共 12 条）
反应条件
1: n-BuLi, HMDS / tetrahydrofuran; hexane / 1.) -78 deg C, 10 min, 2.) -78 deg C to r.t., 30 min
2: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -60 - 0 °C
View Scheme
参考文献
Mouries, Virginie; Waschbuesch, Rachel; Carran, John; Savignac, Philippe
Synthesis, 1998 , # 3 p. 271 - 274
反应条件
1: 87 percent / KOH / toluene / 5 h / Heating
2: 22 percent / dichlorobis(triphenylphosphine)palladium(II); copper(I) chloride; triethylamine / 24 h / 80 °C
View Scheme
参考文献
Umezawa, Hirohito; Okada, Shuji; Oikawa, Hidetoshi; Matsuda, Hiro; Nakanishi, Hachiro
Journal of Physical Organic Chemistry, 2005 , vol. 18, # 5 p. 468 - 472
