2-乙酰氨基-3,4,6-三-O-乙酰基-2-脱氧-Β-D-吡喃葡萄糖酰基叠氮化物合成路线 （共 23 条）
反应条件
sodium azide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate in dichloromethane
参考文献
Shin, Injae; Jung, Hyuk-Jun; Lee, Myung-Ryul
Tetrahedron Letters, 2001 , vol. 42, # 7 p. 1325 - 1328
反应条件
sodium azide in N,N-dimethyl-formamide T=70°C;
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
trimethylsilylazide; tetrabutyl ammonium fluoride in tetrahydrofuran T=65°C; 22 h;
参考文献
Soli, Eric D.; Manoso, Amy S.; Patterson, Michael C.; DeShong, Philip; Favor, David A.; Hirschmann, Ralph; Smith III, Amos B.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3171 - 3177
反应条件
trimethylsilylazide; silver perchlorate; tin(IV) chloride in dichloromethane; toluene 7 h;
参考文献
Matsubara, Koki; Mukaiyama, Teruaki
Chemistry Letters, 1994 , # 2 p. 247 - 250
反应条件
1-methyl-1H-imidazole; zinc in ethyl acetate 6 h; Heating;
参考文献
Tetrahedron Letters, , vol. 45, # 49 p. 9095 - 9097
反应条件
1: 20 °C 2: sodium azide / N,N-dimethyl-formamide / 70 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 732 - 735
反应条件
1.1: sodium methylate / methanol 1.2: 0 - 20 °C 2.1: 20 °C 3.1: sodium azide / N,N-dimethyl-formamide / 70 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 732 - 735
反应条件
1: DIPEA, PDT / CH2Cl2 / 2 h 2: pyridine / 2 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 6 p. 871 - 884
反应条件
1: 95.5 percent / pyridine / 5 h / Ambient temperature 2: 94 percent / Me3SiN3, molecular sieves 3A, SnCl4 / CH2Cl2 / 12 h / Ambient temperature 3: 1.) NaBH4, 2.) pyridine / 1.) CH2Cl2, MeOG, 10 min, 2.) room temperature, 2 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 405 - 416
反应条件
1: 88.5 percent / acetone; H2O / 3 h 2: 95.5 percent / pyridine / 5 h / Ambient temperature 3: 94 percent / Me3SiN3, molecular sieves 3A, SnCl4 / CH2Cl2 / 12 h / Ambient temperature 4: 1.) NaBH4, 2.) pyridine / 1.) CH2Cl2, MeOG, 10 min, 2.) room temperature, 2 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 405 - 416
