1-甲基丙-1-烯基乙酸酯合成路线 (共 10 条)
反应条件
chlorine; dinitrogen tetraoxide in tetrachloromethane
参考文献
Bachman,G.B. et al.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1312 - 1322
参考文献
Young et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3635,3639, 3642
参考文献
Hauser et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3231
反应条件
tetrachloromethane; bromine anschliessend mit Methanol;
参考文献
Parham et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1166,1168
反应条件
(i) Cu, methylcyclohexane, (ii) KOH, MeOH; Multistep reaction;
参考文献
Bernasconi,S. et al.
Synthetic Communications, 1978 , vol. 8, p. 71 - 74
参考文献
Young et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3635,3639, 3642
反应条件
tri-n-butyltin methoxide; bis (triortho-tolylphosphine)palladium(II) chloride in toluene
T=100°C; 5 h;
参考文献
Kosugi, Masanori; Hagiwara, Isao; Sumiya, Takashi; Migita, Toshihiko
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 344 - 345
反应条件
lithium chloride in water; acetone
1.) 2 h, 3 to 10 deg C, 2.) 2 h, 10 deg C to room temp., 3.) 2 h, room temp.;
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069
反应条件
boron trifluoride
T=-20°C; anschliessend Erhitzen mit wss.Natriumacetat;
参考文献
Hauser et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3231
参考文献
Hauser et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3231