4-甲基-N-苯基苯胺合成路线 (共 140 条)
反应条件
copper(l) iodide; 1,10-phenanthroline; sodium t-butanolate in toluene T=20 - 120°C; 40.3333 h;
参考文献
Chemistry - A European Journal, , vol. 17, # 9 p. 2716 - 2723
反应条件
copper; potassium carbonate; polyethylene glycol T=90 - 205°C; 17 h; Heating / reflux;
参考文献
Orient Chemical Industries, Ltd.
Patent: EP1553079 A2, 2005 ;
Location in patent: Page/Page column 11-12 ;
反应条件
1: alcohol; hydrochloric acid; water; sodium nitrite 2: alcohol; diethyl ether; hydrochloric acid / man zerlegt das gefaellte Hydrochlorid durch alkoh. Ammoniak 3: alcoholic ammonium sulfide View Scheme
参考文献
Reichold
Justus Liebigs Annalen der Chemie, 1889 , vol. 255, p. 164
反应条件
sodium dichromate; sulfuric acid; acetic acid T=25°C; anschliessendes Erwaermen mit NaHSO3-Loesung auf 70grad;
参考文献
Wieland; Wecker
Chemische Berichte, 1922 , vol. 55, p. 1810
反应条件
anschliessende Reduktion des olivgruenen Niederschlags mit Disulfitloesung bei 70grad;
参考文献
Wieland; Wecker
Chemische Berichte, 1922 , vol. 55, p. 1810
参考文献
Ishikawa, Wataru; Inada, Hiroshi; Nakano, Hideyuki; Shirota, Yasuhiko
Chemistry Letters, 1991 , # 10 p. 1731 - 1734
反应条件
zinc(II) chloride
T=220 - 230°C;
参考文献
Jensen; Rethwisch
Journal of the American Chemical Society, 1928 , vol. 50, p. 1146
Show Details
Bonna
Justus Liebigs Annalen der Chemie, 1887 , vol. 239, p. 63
反应条件
dibenzoyl peroxide in chloroform
6 h; HeatingIrradiation;
参考文献
Bhattacharyya, Prantosh; Jash, Sagar S.; Dey, Asesh K.
Journal of the Chemical Society, Chemical Communications, 1984 , # 24 p. 1668 - 1669
反应条件
sulfur; iodine in 1,2-dichloro-benzene
T=160°C; 2 h; Heating / reflux;
参考文献
The Regents of the University of California
Patent: US2003/229082 A1, 2003 ;
Location in patent: Page 16 ;
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 2437 - 2441