2-氨基-3,4,5-三甲氧基苯甲酸合成路线 （共 18 条）
反应条件
sodium hydroxide in water; isopropyl alcohol 3 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 6 p. 1701 - 1703
反应条件
hydrogenchloride; tin(ll) chloride T=80°C; 0.333333 h;
参考文献
Liu, Gang; Sun, Lin; Liu, Chunping; Ji, Chunnuan; Wen, Quanwu; Ma, Songmei
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 3 p. 759 - 764
反应条件
1: H2 / 5percent Pd/C (50percent water wet) / propan-2-ol / 8 h / 68 - 75 °C / 2068.6 Torr 2: 50percent aq. NaOH / propan-2-ol; H2O / 3 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 6 p. 1701 - 1703
反应条件
ammonia; potassium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=150°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 13 p. 1483 - 1486
反应条件
1: 4.5 g / H2 / 10percent Pd/C / methanol 2: pyridine / CHCl3 / 0.5 h 3: 200 mg / 1N NaOH / 1 h / 100 °C 4: 10percent NaOH / 4 h View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 4 p. 1005 - 1012
反应条件
1: water containing CHCl3; bromine 2: copper-powder; aqueous NH3 View Scheme
参考文献
Chemische Berichte, , vol. 89, p. 511,517
反应条件
1: pyridine / CHCl3 / 0.5 h 2: 200 mg / 1N NaOH / 1 h / 100 °C 3: 10percent NaOH / 4 h View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 4 p. 1005 - 1012
反应条件
1: nitric acid / acetic acid / 1 h / 20 °C / |Cooling with ice 2: SnCl2·2H2O; hydrogenchloride / ethanol / |Inert atmosphere; |Reflux 3: sodium hydroxide; water / ethanol / 45 - 50 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 69, p. 711 - 718
反应条件
1: 200 mg / 1N NaOH / 1 h / 100 °C 2: 10percent NaOH / 4 h View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 4 p. 1005 - 1012
反应条件
ammonium hydroxide; copper
参考文献
Chemische Berichte, , vol. 89, p. 511,517
