2-溴-4'-甲基苯乙酮合成路线 (共 167 条)
反应条件
N-bromosuccinmide; silica gel in methanol 0.283333 h; Reflux; chemoselective reaction;
参考文献
Mohan Reddy, Bodireddy; Venkata Ramana Kumar, Velpula; Chinna Gangi Reddy, Nallagondu; Mahender Rao, Siripragada
Chinese Chemical Letters, 2014 , vol. 25, # 1 p. 179 - 182
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide in methanol; dichloromethane 2 h; Ambient temperature;
参考文献
Kihara, Masaru; Kashimoto, Minoru; Kobayashi, Yoshimaro; Nagao, Yoshimitsu
Heterocycles, 1992 , vol. 34, # 4 p. 747 - 756
反应条件
water; silver fluoride; trifluoroacetic acid T=40°C; 6 h; Green chemistry;
参考文献
Chen, Zheng-Wang; Ye, Dong-Nai; Ye, Min; Zhou, Zhong-Gao; Li, Shen-Huan; Liu, Liang-Xian
Tetrahedron Letters, 2014 , vol. 55, # 7 p. 1373 - 1375
反应条件
water; [C5mim][BF4] T=125°C; P=2585.74 Torr; 0.0416667 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Chattopadhyay, Kalicharan; Jana, Ranjan
Tetrahedron, 2007 , vol. 63, # 1 p. 155 - 159
反应条件
Sodium bromate; sulfuric acid; sodium bromide in 1,4-dioxane; water T=20°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2529 - 2532
反应条件
dipotassium peroxodisulfate; potassium bromide in water T=60°C; 12 h; Green chemistry;
参考文献
Jiang, Qing; Sheng, Wenbing; Guo, Cancheng
Green Chemistry, 2013 , vol. 15, # 8 p. 2175 - 2179
反应条件
aluminium trichloride in 1,2-dichloro-ethane 4 h; Ambient temperature;
参考文献
Huff, Bret E.; Leffelman, Cindy L.; LeTourneau, Michael E.; Sullivan, Kevin A.; Ward, Jeffrey A.; Stille, John R.
Heterocycles, 1997 , vol. 45, # 7 p. 1363 - 1384
反应条件
N-bromosuccinmide in chloroform T=20°C; 18 h;
参考文献
Synthetic Communications, , vol. 38, # 10 p. 1629 - 1637
反应条件
dihydrogen peroxide in 1,4-dioxane; water T=25°C; 9.5 h;
参考文献
Synthetic Communications, , vol. 40, # 21 p. 3233 - 3239
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=33 - 35°C; 0.25 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 51, # 51 p. 6695 - 6699