2-氨基-4-硝基苯甲酸合成路线 (共 72 条)
反应条件
1: 1.) aq. KOH, 2.) 6 N aq. HCl / 1.) RT, 4 h, 2.) 0 deg C, 90 min 2: 1.) Br2, 1 N aq. KOH, 2.) 2 N aq. HCl / 1.) heating, 1 h, 2.) 0 deg C View Scheme
参考文献
Heterocycles, , vol. 35, # 2 p. 775 - 789
反应条件
ammonium hydroxide Behandeln des entstandenen Gemisches mit alkal. Natriumhypochlorit-Loesung;
参考文献
Journal of the Chemical Society, , vol. 127, p. 1794
反应条件
alkaline aqueous potassium hypobromite
参考文献
Journal of the Chemical Society, , p. 625,627
参考文献
Journal of the American Chemical Society, , vol. 31, p. 847
参考文献
Journal of the American Chemical Society, , vol. 31, p. 847
反应条件
in benzene T=340°C; in sealed tube; other solvent (neat); Product distributionKineticsRate constant;
参考文献
Journal of Physical Chemistry, , vol. 99, # 23 p. 9593 - 9602
反应条件
T=343°C; thermolysis in supercritical benzene; other temperature, pressure; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 56, # 10 p. 3306 - 3314
参考文献
Helvetica Chimica Acta, , vol. 7, p. 906
参考文献
Monatshefte fuer Chemie, , vol. 23, p. 418
Chemische Berichte, , vol. 34, p. 4352
反应条件
1: borane-THF / tetrahydrofuran / 1 h / 0 - 30 °C / |Inert atmosphere 2: manganese(IV) oxide / dichloromethane / 23 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 19 p. 5810 - 5831