咪唑并[1,2-a]吡啶-3-甲醛合成路线 (共 20 条)
反应条件
trichlorophosphate T=100°C; 14 h;
参考文献
Del Corona; Pellegatta; Signorelli; Buran; Massaroli; Turba; Faini; Pagella
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 12 p. 994 - 1003
反应条件
N,N,N',N,-tetramethylethylenediamine; oxygen; silver nitrate in acetonitrile T=60°C; 4 h; Reagent/catalyst;
参考文献
Chandra Mohan, Darapaneni; Nageswara Rao, Sadu; Adimurthy, Subbarayappa
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1266 - 1272
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in water; propionic acid
反应条件
copper dichloride; isopentyl nitrite in acetonitrile T=65°C; Sandmeyer reaction; 0.0833333 h;
参考文献
Chemical Communications, , vol. 47, # 17 p. 5043 - 5045
反应条件
copper dichloride; isopentyl nitrite in acetonitrile T=65°C; 0.5 h;
参考文献
Chemical Communications, , vol. 47, # 17 p. 5043 - 5045
反应条件
[copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; oxygen in N,N-dimethyl-formamide T=105°C; 13 h;
参考文献
Wang, Honggen; Wang, Yong; Liang, Dongdong; Liu, Lanying; Zhang, Jiancun; Zhu, Qiang
Angewandte Chemie - International Edition, 2011 , vol. 50, # 25 p. 5678 - 5681
反应条件
1: trifluoroacetic acid / dichloromethane / 0 °C 2: N-iodo-succinimide / dichloromethane / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 17 p. 5043 - 5045
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 - 5 °C 1.2: 1.5 h / 20 °C 2.1: trifluoroacetic acid / dichloromethane / 0 °C 3.1: N-iodo-succinimide / dichloromethane / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 17 p. 5043 - 5045
反应条件
in 1,4-dioxane 72 h; Heating / reflux;
参考文献
WO2006/128692 A2, ;
Page/Page column 64; 65 ;
反应条件
silver trifluoromethanesulfonate in acetonitrile 2 h; Inert atmosphereReflux; TimeReagent/catalyst;
参考文献
European Journal of Organic Chemistry, , # 1 p. 35 - 39