1,2-二氢-1-苯基-2-硫代烟醛合成路线 （共 9 条）
反应条件
sodium hydroxide; dihydrogen peroxide in water T=35°C; 16 h;
参考文献
Becher, Jan; Johansen, Tea; Michael, Maged Aziz
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 41 - 48
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol; water
1 h; Heating;
参考文献
Becher, Jan; Johansen, Tea; Michael, Maged Aziz
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 41 - 48
反应条件
in acetic anhydride
1) reflux, 10 h, 2) RT, 24 h;
参考文献
Christensen, Mads Chr.; Becher, Jan
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1357 - 1363
反应条件
sodium ethanolate in ethanol
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Michael, Maged Aziz; Becher, Jan; Winckelmann, Ib
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1651 - 1656
反应条件
sodium ethanolate in ethanol
参考文献
Michael, Maged Aziz; Becher, Jan; Winckelmann, Ib
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1651 - 1656
反应条件
1: 83 percent / sodium carbonate, hydroxylamine hydrochloride / ethanol; H2O / 1 h / Heating
2: 52 percent / neutral aluminum oxide / toluene / 2 h / Heating
3: 81 percent / conc. H2SO4 / 24 h / 60 °C
View Scheme
参考文献
Becher, Jan; Johansen, Tea; Michael, Maged Aziz
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 41 - 48
反应条件
hydrogen; molybdenium catalyst T306 in ethanol
T=100°C; P=54720 Torr; 48 h;
参考文献
Becher, Jan; Johansen, Tea; Michael, Maged Aziz
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 41 - 48
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Becher,J.; Frandsen,E.G.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1976 , vol. 30, # 9 p. 863 - 866
反应条件
sulfuric acid in dimethyl sulfoxide
T=80°C; 12 h;
参考文献
Becher, Jan; Johansen, Tea; Michael, Maged Aziz
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 1 p. 41 - 48
