in tetrachloromethane
soln. of ICl (2 mol) in CCl4 added dropwise at 0°C to soln. of (Z)-1-(2-(tribenzylstannyl)vinyl)-1-cycloheptanol (1 mol) in CCl4 with stirring; after addn. of ICl react. mixt. was kept 8 h at room temp.; solvent evapd.; crystn. from cyclohexane/CCl4 (1:1 v/v); elem. anal.;
参考文献
Ren, Yujie; Jia, Cuiying; Liang, Peng; Yang, Xuefeng; Chen, Huilin
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 2003 , vol. 33, # 6 p. 1115 - 1123