4-甲基-2(对甲苯磺酰基)苯乙酮合成路线 (共 21 条)
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=80°C; Kumada Cross-Coupling; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 39 p. 9909 - 9913
反应条件
anhydrous iron chloride; dipotassium peroxodisulfate; oxygen in water
T=20°C; 9 h; Green chemistry;
参考文献
Singh, Atul K.; Chawla, Ruchi; Yadav, Lal Dhar S.
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2845 - 2848
反应条件
T=30°C; 5 h; Ionic liquid;
参考文献
Kumar, Anil; Muthyala, Manoj Kumar
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5368 - 5370
反应条件
silver nitrate in tetrahydrofuran; water
T=20°C; 30 h; Inert atmosphere;
参考文献
Deng, Gui Sheng; Sun, Teng Fei
Chinese Chemical Letters, 2012 , vol. 23, # 10 p. 1115 - 1118,4
反应条件
1: With 2,2'-azo-bisisobutyronitrile in benzene
20 h; Heating;
2: With trifluoroacetic acid
T=50 - 60°C; 10 h;
参考文献
Qian, Hao; Huang, Xian
Synthesis, 2006 , # 12 p. 1934 - 1936
反应条件
(hydroxy(tosyloxy)iodo)benzene; tetrabutyl ammonium fluoride
T=20°C; 0.116667 h;
参考文献
Kumar, Dalip; Sundaree, Swapna; Rao; Varma, Rajender S.
Tetrahedron Letters, 2006 , vol. 47, # 25 p. 4197 - 4199
反应条件
lt;Ru(PPh3)3Cl2gt; in benzene
T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
water; toluene-4-sulfonic acid in tetrahydrofuran
T=50°C; 48 h;
参考文献
Lai, Chunbo; Xi, Chanjuan; Jiang, Yanfeng; Hua, Ruimao
Tetrahedron Letters, 2005 , vol. 46, # 3 p. 513 - 515
反应条件
PEG-400
T=20°C; 0.166667 h;
参考文献
Suryakiran; Reddy, T. Srikanth; Ashalatha; Lakshman; Venkateswarlu
Tetrahedron Letters, 2006 , vol. 47, # 23 p. 3853 - 3856