potassium phosphate; chlorobenzene; palladium diacetate; 2-dicyclohexylphosphino-1,1'-biphenyl in toluene
T=105°C; 24 h; Under Artoluene soln. of aldehyde, amine and PhCl then toluene soln. of Pd-compd. and P-compd. were added to K3PO4;
参考文献
Symyx Technologies, Inc.
Patent: US6339157 B1, 2002 ;
Location in patent: Example 5 ;
MPEG-supported benzyldiisopropylamine in dichloromethane
T=25°C; 6 h; Inert atmosphere;
参考文献
Figlus, Marek; Tarruella, Albert C.; Messer, Anastasia; Sollis, Steven L.; Hartley, Richard C.
Chemical Communications, 2010 , vol. 46, # 24 p. 4405 - 4407
triethylamine; PdCl2(PMePh2)2 in neat (no solvent)
T=100°C; P=7600 Torr; 72 h;
参考文献
Ozawa, Fumiyuki; Soyama, Hidehiko; Yanagihara, Hisayoshi; Aoyama, Issei; Takino, Hiroaki; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 11 p. 3235 - 3245
