顺式-4-羟基-L-脯氨酸合成路线 （共 45 条）
反应条件
1: dimethylsulfoxide / 20 - 50 °C 2: 38 percent / diethylaminosulfur trifluoride / CH2Cl2 / 20 h / 0 - 20 °C 3: 22 percent / water / propan-2-ol / 48 h / 20 °C View Scheme
参考文献
Hamacher, Kurt
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1135 - 1144
反应条件
1: dimethylsulfoxide / 20 - 50 °C 2: 38 percent / diethylaminosulfur trifluoride / CH2Cl2 / 20 h / 0 - 20 °C 3: 22 percent / water / propan-2-ol / 48 h / 20 °C View Scheme
参考文献
Hamacher, Kurt
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1135 - 1144
反应条件
1: dimethylsulfoxide / 20 - 50 °C 2: 38 percent / diethylaminosulfur trifluoride / CH2Cl2 / 20 h / 0 - 20 °C 3: 22 percent / water / propan-2-ol / 48 h / 20 °C View Scheme
参考文献
Hamacher, Kurt
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1135 - 1144
反应条件
thionyl chloride
T=20°C;
参考文献
Orliac, Aurelie; Routier, Julie; Burgat Charvillon, Fabienne; Sauer, Wolfgang H. B.; Bombrun, Agnes; Kulkarni, Santosh S.; Gomez Pardo, Domingo; Cossy, Janine
Chemistry - A European Journal, 2014 , vol. 20, # 13 p. 3813 - 3824
反应条件
1: NaHCO3
2: methanol
3: LiBH4 / tetrahydrofuran
View Scheme
参考文献
Ceulemans, G.; Aerschot, A. Van; Herdewijn, P.
Collection of Czechoslovak Chemical Communications, 1996 , vol. 61, p. S234 - S237
