暂无反应条件数据

potassium tert-butylate; potassium iodide in tert-butyl alcohol 1.) room temp., 1-2 h; 2.) reflux, 22-24 h;

toluene

1: 65 percent / KOH / aq. ethanol / 12 h / Heating 2: 1.) Hg(OAc)2; 2.) NaBH4, aq. NaOH / 1.) H2O, THF, room temp., 10 min; 2.) 10 min, ice/water bath 3: 65 percent / n-butyl nitrite, aq. HCl / aq. ethanol / 6 h View Scheme