2,3-丁烷二酮单(O-甲基肟)合成路线 (共 6 条)
参考文献
Ceresole
Chemische Berichte, 1883 , vol. 16, p. 834
反应条件
hydrogenchloride
T=60°C;
参考文献
Thilo
Chemische Berichte, 1929 , vol. 62, p. 869
参考文献
Diels; Stern
Chemische Berichte, 1907 , vol. 40, p. 1624
反应条件
1: aqueous-alcoholic KOH-solution; hydroxylamine hydrochloride
2: hydrochloric acid / 60 °C
View Scheme
参考文献
Thilo
Chemische Berichte, 1929 , vol. 62, p. 869
参考文献
Thilo
Chemische Berichte, 1929 , vol. 62, p. 869
反应条件
anhydrous ammonium carbonate; water in ethanol
T=70°C; 20 h;
参考文献
Bowness, W. Gary; Howe, Ralph; Rao, Balbir S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2649 - 2653