3,4-二异丙氧基-3-环丁烯-1,2-二酮合成路线 （共 12 条）
反应条件
in benzene 72 h; Heating;
参考文献
Liebeskind, Lanny S.; Fengl, Richard W.; Wirtz, Kevin R.; Shawe, Thomas T.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2482 - 2488
反应条件
in diethyl ether 1) reflux, 2 h, 2) room temp., 18 h;
参考文献
Dehmlow, Eckehard V.; Schell, Hans G.
Chemische Berichte, 1980 , vol. 113, # 1 p. 1 - 8
参考文献
Liu, Hiu; Tomooka, Craig S.; Moore, Harold W.
Synthetic Communications, 1997 , vol. 27, # 12 p. 2177 - 2180
反应条件
in isopropyl alcohol Reflux;
参考文献
Australian Journal of Chemistry, , vol. 63, # 12 p. 1656 - 1664
反应条件
in 2,2,4-trimethylpentane T=25°C; Irradiation; Kinetics;
参考文献
Journal of Organic Chemistry, , vol. 73, # 5 p. 1768 - 1773
参考文献
Fu, Nanyan; Allen, Annette D.; Kobayashi, Shinjiro; Tidwell, Thomas T.; Vukovic, Sinisa; Matsuoka, Takeshi; Mishima, Masaaki
Journal of Organic Chemistry, 2008 , vol. 73, # 5 p. 1768 - 1773
反应条件
n-Bu4N+CN- in tetrahydrofuran T=-23°C;
参考文献
PARATEK PHARMACEUTICALS, INC.; OAK, K., Kim
Patent: WO2008/79363 A2, 2008 ;
Location in patent: Page/Page column 34 ;
反应条件
lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=-20°C;
参考文献
Liebeskind, Lanny S.; Wirtz, Kevin R.
Journal of Organic Chemistry, 1990 , vol. 55, # 19 p. 5350 - 5358
反应条件
in tetrahydrofuran; diethyl ether; hexane
参考文献
Imperial Chemical Industries PLC
Patent: US5254683 A1, 1993 ;
反应条件
hydrogenchloride in water; isopropyl alcohol
3 h; Inert atmosphereReflux;
参考文献
Wang, Siyi; Hall, Lincoln; Diev, Vyacheslav V.; Haiges, Ralf; Wei, Guodan; Xiao, Xin; Djurovich, Peter I.; Forrest, Stephen R.; Thompson, Mark E.
Chemistry of Materials, 2011 , vol. 23, # 21 p. 4789 - 4798
