5-甲氧基-3-(2-硝基乙烯基)-吲哚合成路线 （共 9 条）
反应条件
ammonium acetate in benzene Henry reaction; Reflux;
参考文献
Zhang, Pu Yong; Wan, Sheng Biao; Ren, Su Mei; Jiang, Tao
Chinese Chemical Letters, 2010 , vol. 21, # 11 p. 1307 - 1309
反应条件
1: POCl3 / 0 °C 2: NH4OAc / 70 °C View Scheme
参考文献
Archiv der Pharmazie, , vol. 338, # 2-3 p. 67 - 73
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Heating;
参考文献
Archiv der Pharmazie, , vol. 338, # 2-3 p. 67 - 73
Pharmazie, , vol. 60, # 9 p. 643 - 647
反应条件
1: diethyl ether; tetrahydrofuran / 3 h / -50 - 0 °C 2: HCO2NH4 / Pd/C / methanol / 80 °C View Scheme
参考文献
Trujillo, John I.; Meyers, Marvin J.; Anderson, David R.; Hegde, Shridhar; Mahoney, Matthew W.; Vernier, William F.; Buchler, Ingrid P.; Wu, Kun K.; Yang, Syaluan; Hartmann, Susan J.; Reitz, David B.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 16 p. 4657 - 4663
反应条件
hydrogen; nickel in tetrahydrofuran P=3040 Torr; 10 h; Ambient temperature;
参考文献
Spadoni, Gilberto; Balsamini, Cesarino; Diamantini, Giuseppe; Di Giacomo, Barbara; Tarzia, Giorgio; Mor, Marco; Plazzi, Pier Vincenzo; Rivara, Silvia; Lucini, Valeria; Nonno, Romolo; Pannacci, Marilou; Fraschini, Franco; Stankov, Bojidar Michaylov
Journal of Medicinal Chemistry, 1997 , vol. 40, # 13 p. 1990 - 2002
反应条件
1: LiAlH4 / tetrahydrofuran / Heating 2: Et3N / tetrahydrofuran / 6 h / 20 °C View Scheme
参考文献
Ates-Alagoz; Buyukbingol; Buyukbingol, Erdem
Pharmazie, 2005 , vol. 60, # 9 p. 643 - 647
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C 2: hydrogenchloride / methanol / 20 °C 3: manganese(IV) oxide; 5 Pd(II)/C(eggshell) / N,N-dimethyl-formamide / 150 °C / Microwave irradiation View Scheme
参考文献
Cuny, Gregory D.; Ulyanova, Natalia P.; Patnaik, Debasis; Liu, Ji-Feng; Lin, Xiangjie; Auerbach, Ken; Ray, Soumya S.; Xian, Jun; Glicksman, Marcie A.; Stein, Ross L.; Higgins, Jonathan M.G.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 5 p. 2015 - 2019
反应条件
1: LiAlH4 / tetrahydrofuran / Heating
2: 31 percent / Et3N / tetrahydrofuran / 6 h / 20 °C
View Scheme
参考文献
Ates-Alagoz; Buyukbingol; Buyukbingol, Erdem
Pharmazie, 2005 , vol. 60, # 9 p. 643 - 647
反应条件
sodium tetrahydroborate in tetrahydrofuran; methanol
T=20°C;
参考文献
Zhang, Pu Yong; Wan, Sheng Biao; Ren, Su Mei; Jiang, Tao
Chinese Chemical Letters, 2010 , vol. 21, # 11 p. 1307 - 1309
