water in dichloromethane (N2); addn. of HBBr2(SMe2) at 0°C; filtration after 12 h into mixture of ice and ether (1:1); stirring for 30 min at room temperature; washing of organic phase with satd. NaCl-soln.; drying (MgSO4); removal of solvent in vac.; washing with hexane;
参考文献
Jego, Jean Michel; Carboni, Bertrand; Vaultier, Michel; Carrie, Robert
Journal of the Chemical Society, Chemical Communications, 1989 , # 2 p. 142 - 143
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 25, p. 2153 - 2159
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 25, p. 2308 - 2315
Jego, Jean Michel; Carboni, Bertrand; Vaultier, Michel; Carrie, Robert
Journal of the Chemical Society, Chemical Communications, 1989 , # 2 p. 142 - 143
Vasilev,L.S. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 2153 - 2159
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, p. 2308 - 2315
(i) KOH, (ii) /BRN= 969148/, benzene; Multistep reaction;
参考文献
Vasilev,L.S. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, p. 2153 - 2159
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, p. 2308 - 2315
