反应条件
1: 93 percent / sulfuric acid / 16 h / Heating 2: 77 percent / sodium hydrocarbonate / acetone / 16 h / Heating 3: hydrogen / Pd/C / methanol; tetrahydrofuran / 16 h / 20 °C 4: 700 mg / acetic acid / methanol; tetrahydrofuran / 0.5 h / Heating 5: 87 percent / BF3*Et2O; sodium borohydride / tetrahydrofuran / 2 h View Scheme
参考文献
Walker, Daniel P.; Wishka, Donn G.; Piotrowski, David W.; Jia, Shaojuan; Reitz, Steven C.; Yates, Karen M.; Myers, Jason K.; Vetman, Tatiana N.; Margolis, Brandon J.; Jacobsen, E. Jon; Acker, Brad A.; Groppi, Vincent E.; Wolfe, Mark L.; Thornburgh, Bruce A.; Tinholt, Paula M.; Cortes-Burgos, Luz A.; Walters, Rodney R.; Hester, Matthew R.; Seest, Eric P.; Dolak, Lester A.; Han, Fusen; Olson, Barbara A.; Fitzgerald, Laura; Staton, Brian A.; Raub, Thomas J.; Hajos, Mihaly; Hoffmann, William E.; Li, Kai S.; Higdon, Nicole R.; Wall, Theron M.; Hurst, Raymond S.; Wong, Erik H.F.; Rogers, Bruce N.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 24 p. 8219 - 8248
