1,2-二甲基-3,5-二硝基苯合成路线 （共 18 条）
反应条件
sulfuric acid; nitric acid
T=0°C; 24 h;
参考文献
Medina, Inmaculada C. Rodriguez; Hanson, James R.
Journal of Chemical Research, Synopses, 2003 , # 5 p. 303 - 304
反应条件
nitrogen(IV) oxide; ozone in dichloromethane
T=-10°C; 3 h;
参考文献
Suzuki, Hitomi; Murashima, Takashi; Kozai, Iku; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1591 - 1598
反应条件
1: 23 percent / methanol
2: 58 percent / boron trifluoride-etherate / 1.2 h / 0 °C
3: 1) nitric acid, acetic anhydride, trifluoroacetic acid / 1) 0 deg C, 5 min, 2) acetic anhydride, 0 deg C, 2 h
View Scheme
参考文献
Fischer, Alfred; Henderson, George N.; Iyer, Lokanathan M.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 2390 - 2400
反应条件
sulfuric acid
T=35°C; 18 h;
参考文献
Fischer, Alfred; Henderson, George N.; Iyer, Lokanathan M.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 2390 - 2400
参考文献
Borsche; Fiedler
Chemische Berichte, 1913 , vol. 46, p. 2125
反应条件
sulfuric acid; nitric acid
参考文献
Crossley; Renouf
Journal of the Chemical Society, 1909 , vol. 95, p. 208
Full Text Show Details
Noelting; Thesmar
Chemische Berichte, 1902 , vol. 35, p. 632
反应条件
1: 58 percent / boron trifluoride-etherate / 1.2 h / 0 °C
2: 1) nitric acid, acetic anhydride, trifluoroacetic acid / 1) 0 deg C, 5 min, 2) acetic anhydride, 0 deg C, 2 h
View Scheme
参考文献
Fischer, Alfred; Henderson, George N.; Iyer, Lokanathan M.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 2390 - 2400
反应条件
1: diethyl ether
2: acetic acid; sulfuric acid
3: water
View Scheme
参考文献
Borsche; Fiedler
Chemische Berichte, 1913 , vol. 46, p. 2125
反应条件
1: acetic acid; sulfuric acid
2: water
View Scheme
参考文献
Borsche; Fiedler
Chemische Berichte, 1913 , vol. 46, p. 2125
反应条件
sulfuric acid; nitric acid
参考文献
Noelting; Thesmar
Chemische Berichte, 1902 , vol. 35, p. 632
