反应条件
1.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C / |Inert atmosphere
1.2: 1 h / 20 °C / |Inert atmosphere
2.1: 1,1,2,2-tetramethylethylene; potassium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 0.73 h / 20 °C
3.1: sulfuric acid / 2 h / |Reflux
View Scheme
参考文献
Windsor, Matthew A.; Hermanson, Daniel J.; Kingsley, Philip J.; Xu, Shu; Crews, Brenda C.; Ho, Winnie; Keenan, Catherine M.; Banerjee, Surajit; Sharkey, Keith A.; Marnett, Lawrence J.
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 9 p. 759 - 763