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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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61541-61-5
合成路线
（共 7 条）
75-15-0
二硫化碳
+
121-97-1
4'-甲氧基苯丙酮
+
74-88-4
甲基碘
→
反应条件
61541-61-5
反应条件
(i) NaOtBu, benzene, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Chauhan,S.M.S.; Junjappa,H.
Tetrahedron, 1976 , vol. 32, p. 1911 - 1916
61541-59-1
+
61541-61-5
→
反应条件
82238-79-7
+
89003-23-6
+
89003-22-5
+
89003-24-7
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
61541-59-1
+
61541-61-5
→
反应条件
82238-79-7
+
89003-23-6
+
89003-22-5
+
89003-24-7
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
61541-59-1
+
61541-61-5
→
反应条件
82238-82-2
+
89003-22-5
+
89003-24-7
+
89003-25-8
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
61541-59-1
+
61541-61-5
→
反应条件
89003-23-6
+
89003-22-5
+
89003-24-7
+
89003-25-8
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
61541-59-1
+
61541-61-5
→
反应条件
82238-79-7
+
89003-23-6
+
89003-22-5
+
89003-24-7
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
61541-59-1
+
61541-61-5
→
反应条件
89003-23-6
+
89003-22-5
+
89003-24-7
+
89003-25-8
反应条件
sodium hydride in N,N-dimethyl-formamide T=50 - 55°C; 3 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Apparao, Satyam; Ila, Hiriyakkanavar; Junjappa, Hirijakkanavar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2837 - 2844
