2,3:5,6-二-O-环亚己基-Alpha-D-甘露糖合成路线 (共 6 条)
反应条件
sulfuric acid in 1,4-dioxane 0.5 h;
参考文献
Karkishchenko, N. N.; Alekseev, V. G.; Anisimova, V. A.; Korol', E. L.; Vilkov, G. A.; et al.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 4 p. 242 - 247
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 4 p. 408 - 413
参考文献
Russian Journal of General Chemistry, , vol. 66, # 4 p. 680 - 681
Zhurnal Obshchei Khimii, , vol. 66, # 4 p. 697 - 698
反应条件
1: 38 percent / yellow HgO; HgCl2 / acetone; H2O / 3.33 h / 40 - 50 °C 2: sodium methoxide / methanol / 12 h / cooling View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 74, # 2 p. 225 - 229
反应条件
1: 42 percent / aq. H2SO4 / dioxane / 14 h / 20 °C 2: 73 percent / pyridine / 12 h / 20 °C 3: 38 percent / yellow HgO; HgCl2 / acetone; H2O / 3.33 h / 40 - 50 °C 4: sodium methoxide / methanol / 12 h / cooling View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 74, # 2 p. 225 - 229
反应条件
1: 42 percent / aq. H2SO4 / dioxane / 14 h / 20 °C 2: 73 percent / pyridine / 12 h / 20 °C 3: 38 percent / yellow HgO; HgCl2 / acetone; H2O / 3.33 h / 40 - 50 °C 4: sodium methoxide / methanol / 12 h / cooling View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 74, # 2 p. 225 - 229
反应条件
1: 73 percent / pyridine / 12 h / 20 °C 2: 38 percent / yellow HgO; HgCl2 / acetone; H2O / 3.33 h / 40 - 50 °C 3: sodium methoxide / methanol / 12 h / cooling View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 74, # 2 p. 225 - 229