4-(甲苯-4-磺酰基)-2-丁酮合成路线 （共 7 条）
反应条件
anhydrous iron chloride; chloro-trimethyl-silane in dichloromethane
T=20°C;
参考文献
Sreedhar; Reddy, M. Amamath; Reddy, P. Surendra
Synlett, 2008 , # 13 p. 1949 - 1952
反应条件
sodium methylate; boron trifluoride diethyl etherate; trifluoroacetic acid; mercury(II) oxide in dichloromethane
参考文献
Barre, V.; Massias, F.; Uguen, D.
Tetrahedron Letters, 1989 , vol. 30, # 52 p. 7389 - 7392
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 2 h; Further byproducts given;
参考文献
Kamigata, Nobumasa; Satoh, Akira; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 121 - 130
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 2 h; Further byproducts given;
参考文献
Kamigata, Nobumasa; Satoh, Akira; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 121 - 130
参考文献
du Pont de Nemours and Co.
Patent: US2010828 , 1932 ;
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran
T=0 - 20°C; 0.833333 h;
参考文献
Yan, Tu-Hsin; Tsai, Chia-Chung; Chien, Ching-Ting; Cho, Chia-Ching; Huang, Pei-Chen
Organic Letters, 2004 , vol. 6, # 26 p. 4961 - 4963
反应条件
methyllithium
1) hexane, Et2O, 3 h, 2) Et2O, 6 h; Yield given. Multistep reaction;
参考文献
Clennan, E. L.; Yang, Kang
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4477 - 4487
