2-(4-苯甲氧基苯基)乙醇合成路线 (共 40 条)
反应条件
1: With lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 2: With water in diethyl ether
参考文献
AUSPEX PHARMACEUTICALS, INC.
Patent: WO2007/139923 A1, 2007 ;
Location in patent: Page/Page column 77 ;
WO 2007/139923 A1
反应条件
potassium carbonate in acetone 18 h; Heating;
参考文献
Chu, Guo-Hua; Milano, Shawn; Kluth, Lisa; Rhodes, Michael; Boni, Riccardo; Johnson, David A.; Li, Pui-Kai
Steroids, 1997 , vol. 62, # 7 p. 530 - 535
反应条件
potassium carbonate in N,N-dimethyl-formamide T=65°C; 24 h;
参考文献
Aberle, Nicholas; Catimel, Jenny; Nice, Edouard C.; Watson, Keith G.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 13 p. 3741 - 3744
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=20°C; 4 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; ethanol; water T=20°C; 3 h;
参考文献
Fernandes, Rodney A; Bodas, Mandar S; Kumar, Pradeep
Tetrahedron, 2002 , vol. 58, # 6 p. 1223 - 1227
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Manoury; Binet; Rousseau; Lefevre-Borg; Cavero
Journal of Medicinal Chemistry, 1987 , vol. 30, # 6 p. 1003 - 1011
反应条件
borane in tetrahydrofuran
参考文献
Neubert, M. E.; Citano, C. M.; Ezenyilimba, M. C.; Jirousek, M. R.; Sabol-Keast, S.; Sharma, R. B.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 206, p. 103 - 116
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating;
参考文献
Zhou, Feng-Yan; She, Jin; Wang, Yan-Guang
Carbohydrate Research, 2006 , vol. 341, # 15 p. 2469 - 2477
反应条件
in diethyl ether; ethyl acetate
反应条件
1: K2CO3 / dimethylformamide 2: LiBH4 / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 4 p. 525 - 528
反应条件
1: 92.2 percent / K2CO3 / acetone / 10 h / Heating 2: 85 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 341, # 15 p. 2469 - 2477