3-(4-甲氧基苯基)异噁唑合成路线 （共 10 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexanes T=0°C; 1 h; Inert atmosphere;
参考文献
Tetrahedron, , vol. 64, # 49 p. 11198 - 11204
反应条件
1: With TsNHOH; potassium carbonate in methanol; water
T=20°C; 10 h;
2: With potassium carbonate in methanol; water
T=60°C; 4 h; regioselective reaction;
参考文献
Tang, Shibing; He, Jinmei; Sun, Yongquan; He, Liuer; She, Xuegong
Organic Letters, 2009 , vol. 11, # 17 p. 3982 - 3985
反应条件
pyridine; hydroxylamine hydrochloride in ethanol
T=78°C; 16 h;
参考文献
Rosa, Fernanda A.; Machado, Pablo; Bonacorso, Helio G.; Zanatta, Nilo; Martins, Marcos A. P.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 3 p. 879 - 885
反应条件
1: With triethylamine in chloroform
T=20°C; 12 h;
2: With dihydrogen peroxide in chloroform
T=20°C; 0.333333 h;
参考文献
Sheng, Shou-Ri; Liu, Xiao-Ling; Xu, Qu; Song, Cai-Sheng
Synthesis, 2003 , # 18 p. 2763 - 2764
反应条件
1.1: N-chlorosuccinimide / CHCl3 / 0.33 h / 20 °C
2.1: Et3N / CHCl3 / 12 h / 20 °C
2.2: aq. H2O2 / CHCl3 / 0.33 h / 20 °C
View Scheme
参考文献
Sheng, Shou-Ri; Liu, Xiao-Ling; Xu, Qu; Song, Cai-Sheng
Synthesis, 2003 , # 18 p. 2763 - 2764
反应条件
1: With triethylamine in trichloroethane, 1,1,2-
0.5 h; Heating;
2: With sodium hydroxide
0.5 h; Heating;
参考文献
Schofield, Mark H.; Sorel, Marie-Adele; Manalansan, Ryan J.; Richardson, David P.; Markgraf, J. Hodge
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 9 p. 851 - 855
参考文献
Shvekhgeimer,G.A. et al.
Synthesis, 1976 , p. 612 - 614
反应条件
in benzene
Ambient temperaturereaction of other dipolarophiles with different 1,3-dipoles, effect of solvent polarity; Product distribution;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
反应条件
in benzene
2 h; Heating;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
反应条件
in benzene
Ambient temperature;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
