2,2,6,6-四甲基-1-哌啶胺合成路线 （共 10 条）
反应条件
tert-butylhypochlorite; triethylamine 1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
反应条件
tert-butylhypochlorite; triethylamine 1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
反应条件
tert-butylhypochlorite; triethylamine 1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
反应条件
tert-butylhypochlorite; triethylamine 1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
反应条件
lithium aluminium tetrahydride in diethyl ether; anhydrous butyl ether
T=95°C; 4 h;
参考文献
Hinsberg, William D.; Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 766 - 773
反应条件
1: 98 percent / aq. HCl; NaNO2 / 75 - 100 °C
2: 73 percent / LiAlH4 / dibutyl ether / 3 h / 95 °C
View Scheme
参考文献
Lucarini, Marco; Pedulli, Gian Franco; Lazzari, Dario
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2723 - 2727
反应条件
tert-butylhypochlorite; triethylamine
1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
反应条件
tert-butylhypochlorite; triethylamine
1.) Et2O, -78 degC, 1 h, 2.) CCl3F, irradiation, 12 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6660 - 6668
参考文献
Lunazzi, Lodovico; Macciantelli, Dante
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 604 - 609
参考文献
Lunazzi, Lodovico; Macciantelli, Dante
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 604 - 609
