in benzene under N2 atm. pyridine was added to soln. ((EtH2N)B8H11NHEt) in benzene and soln. was heated at reflux for 3 h; volatile components were removed in vacuo, residue was redissolved in CH2Cl2 and chromed.;
参考文献
Journal of Organometallic Chemistry, , vol. 614-615, p. 215 - 222
in benzene
under N2 atm. NHEt2 was added to soln. ((EtH2N)B8H11NHEt) in benzene andheated at reflux for 3 h; volatile components were removed in vacuo, residue was redissolved in CH2Cl2 and chromed.;
参考文献
Doerfler, Udo; Bauer, Claudia; Gabel, Detlef; Rath, Nigam P.; Barton, Lawrence; Kennedy, John D.
Journal of Organometallic Chemistry, 2000 , vol. 614-615, p. 215 - 222
