4-甲基-2(H)-呋喃酮合成路线 (共 53 条)
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0°C; 2 h;
参考文献
Sharma, Vasudha; Kelly, Gilbert T.; Watanabe, Coran M. H.
Organic Letters, 2008 , vol. 10, # 21 p. 4815 - 4818
反应条件
1: methyllithium With iron(III) chloride in diethyl ether cooling; 2: trifluoromethanesulfonic acid 5-oxo-2,5-dihydrofuran-3-yl ester in tetrahydrofuran T=-30°C;
参考文献
Fuerstner, Alois; Martin, Ruben; Krause, Helga; Seidel, Guenter; Goddard, Richard; Lehmann, Christian W.
Journal of the American Chemical Society, 2008 , vol. 130, # 27 p. 8773 - 8787
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=60°C; P=760.051 Torr; 20 h;
参考文献
Greco, George E.; Gleason, Brittany L.; Lowery, Tiffany A.; Kier, Matthew J.; Hollander, Lisa B.; Gibbs, Shoshanah A.; Worthy, Amanda D.
Organic Letters, 2007 , vol. 9, # 19 p. 3817 - 3820
反应条件
triphenylphosphine; (η3-allyl)(η5-Cp)Pd in N,N-dimethyl-formamide T=165°C; P=30002.4 Torr; 2 h; Further byproducts given;
参考文献
Chemische Berichte, , vol. 117, # 2 p. 654 - 665
参考文献
Jeon, Hye-Sun; Yeo, Jung Eun; Jeong, Young Cheol; Koo, Sangho
Synthesis, 2004 , # 17 p. 2813 - 2820
反应条件
silver trifluoromethanesulfonate in toluene T=20°C; 0.5 h; Inert atmosphere;
参考文献
Egi, Masahiro; Ota, Yuya; Nishimura, Yuka; Shimizu, Kaori; Azechi, Kenji; Akai, Shuji
Organic Letters, 2013 , vol. 15, # 16 p. 4150 - 4153
反应条件
1-methyl-pyrrolidin-2-one; iron (III) acetylacetonate in tetrahydrofuran T=-30°C;
参考文献
Scheiper, Bodo; Bonnekessel, Melanie; Krause, Helga; Fuerstner, Alois
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3943 - 3949
反应条件
toluene-4-sulfonic acid in dichloromethane T=20°C; 0.5 h;
参考文献
Saalfrank, Rolf W.; Hafner, Wieland; Markmann, Joachim; Welch, Andreas; Peters, Karl; Schnering, Hans Georg von
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1994 , vol. 49, # 3 p. 389 - 406
反应条件
Rh2(Piv)4 in dichloromethane T=-50°C; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 26 p. 11035 - 11043
反应条件
sodium peroxodisulphate; silver nitrate; copper(II) sulfate in water; acetonitrile T=80°C;
参考文献
Tetrahedron Letters, , vol. 26, # 9 p. 1209 - 1212