(3-氯丙基)三(1-甲基乙氧基)-硅烷合成路线 (共 3 条)
反应条件
triethylamine in diethyl ether
T=20°C; 2 h;
参考文献
Besson, Eric; Mehdi, Ahmad; Lerner, Dan A.; Reye, Catherine; Corriu, Robert J. P.
Journal of Materials Chemistry, 2005 , vol. 15, # 7 p. 803 - 809
反应条件
Aliquatreg; 336 in water; toluene
T=20 - 82°C; 11.6167 h;
参考文献
Cruse, Richard W.; Gonzalez, Leda N.; Himmeldirk, Rodica; Divins, Larry Allen; Jackson, Melinda
Patent: US2005/245753 A1, 2005 ;
Location in patent: Page/Page column 23 ;
反应条件
1: 89 percent / NaN3 / dimethylformamide / 3 h / 60 °C
2: 99 percent / H2 / Pd/C / methanol / 2 h / atmospheric pressure
View Scheme
参考文献
Bianco, Alberto; Maggini, Michele; Nogarole, Marco; Scorrano, Gianfranco
European Journal of Organic Chemistry, 2006 , # 13 p. 2934 - 2941