4-(反-4-丙基环己基)苯腈合成路线 （共 17 条）
反应条件
1: AlCl3 / 1,2-dichloro-ethane / 0.5 h 2: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 3: SOCl2 / 1 h / Heating 4: 25percent aq. NH4OH 5: 56 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 2: SOCl2 / 1 h / Heating 3: 25percent aq. NH4OH 4: 56 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: SOCl2 / 1 h / Heating 2: 25percent aq. NH4OH 3: 56 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / or in 1:1 mixture of triethanolamine and glycerol 2: AlCl3 / 1,2-dichloro-ethane / 0.5 h 3: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 4: SOCl2 / 1 h / Heating 5: 25percent aq. NH4OH 6: 56 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
1: 25percent aq. NH4OH 2: 56 percent / SOCl2, dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674
反应条件
sulfuric acid; water 5 h; Heating;
参考文献
Liang, J. C.; Chen, L.
Molecular Crystals and Liquid Crystals (1969-1991), 1989 , vol. 167, p. 253 - 258
反应条件
magnesium in tetrahydrofuran; diethyl ether
5 h; Heating; Yield given;
参考文献
Osman; Huynh-Ba
Molecular crystals and liquid crystals, 1984 , vol. 116, # 1-2 p. 141 - 152
