4-甲基-2-硝基-N-乙酰基苯胺合成路线 (共 46 条)
反应条件
Bi(NO3)3·5H2O in dichloromethane T=23°C; regioselective reaction;
参考文献
Lu, Yang; Li, Yaming; Zhang, Rong; Jin, Kun; Duan, Chunying
Tetrahedron, 2013 , vol. 69, # 45 p. 9422 - 9427
反应条件
MOA; water; nitric acid in chloroform Nitration; 6 h; Heating;
参考文献
Sana, Sariah; Rajanna; Ali, Mir Moazzam; Saiprakash
Chemistry Letters, 2000 , # 1 p. 48 - 49
参考文献
Porcal, Williams; Merlino, Alicia; Boiani, Mariana; Gerpe, Alejandra; Gonzalez, Mercedes; Cerecetto, Hugo
Organic Process Research and Development, 2008 , vol. 12, # 2 p. 156 - 162
反应条件
nitric acid in acetic anhydride T=-40°C;
参考文献
Fischer, Alfred; Fyles, Deborah L.; Henderson, George N.
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 513 - 514
参考文献
Journal of the American Chemical Society, , vol. 51, p. 1804
反应条件
1: acetic acid / 0.25 h / Heating 2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
n-ethyl morpholine in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 60, # 25 p. 8294 - 8304
反应条件
in tetrachloromethane T=33°C; 0.566667 h;
参考文献
Tanno, Masayuki; Sueyoshi, Shoko
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 4 p. 1360 - 1371
反应条件
nitric acid T=-40°C;
参考文献
Fischer, Alfred; Fyles, Deborah L.; Henderson, George N.
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 513 - 514
反应条件
sulfuric acid; nitric acid
参考文献
Chemische Berichte, , vol. 17, p. 265