N-甲基-N-(4-甲基苯基)乙酰胺合成路线 （共 23 条）
反应条件
triethylsilane; indium tribromide in chloroform T=60°C; 15 h; Inert atmosphere;
参考文献
Sakai, Norio; Fujii, Kohji; Konakahara, Takeo
Tetrahedron Letters, 2008 , vol. 49, # 48 p. 6873 - 6875
反应条件
1: 4-methyl-acetanilide With lithium hexamethyldisilazane in tetrahydrofuran
T=0 - 20°C; 0.5 h; Inert atmosphere;
2: methyl iodide in tetrahydrofuran
Inert atmosphere;
参考文献
McLeod, David; McNulty, James
European Journal of Organic Chemistry, 2012 , # 31 p. 6127 - 6131,5
Title/Abstract Full Text Show Details
McLeod, David; McNulty, James
European Journal of Organic Chemistry, 2012 , # 31 p. 6127 - 6131
反应条件
copper(l) chloride in chlorobenzene
T=130°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Qinqin; Liu, Xiaolong; Zhang, Yuejiao; Chen, Chao; Chen, Wanzhi
Organic Letters, 2013 , vol. 15, # 13 p. 3326 - 3329
反应条件
pyridine; tert.-butylhydroperoxide; iron(II) chloride in acetonitrile
T=85°C; 2 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Ma, Lina; Jia, Fan; Li, Zhiping
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5638 - 5646
反应条件
1: tert-butyl N-p-tolyl-N-methylcarbamate With (μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7; dimethylphenylsilane in ethylene glycol dimethyl ether
T=40°C; 7 h; Inert atmosphere;
2: acetyl chloride With triethylamine in diethyl ether
T=0°C; 1 h; Inert atmosphere;
参考文献
Hanada, Shiori; Yuasa, Akihiro; Kuroiwa, Hirotaka; Motoyama, Yukihiro; Nagashima, Hideo
European Journal of Organic Chemistry, 2010 , # 6 p. 1021 - 1025
反应条件
oxygen; copper(l) chloride in acetonitrile
T=30°C; P=760 Torr; 20 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
oxygen in acetonitrile
T=30°C; P=760 Torr; 4 h; other aromatic and aliphatic tert. amines, other anhydrides, other reaction times, influence of BHT, (effect of concentration of) other metal chlorides, effect of anhydride concentration; Product distributionMechanism;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
oxygen; copper(l) chloride in acetonitrile
T=30°C; P=760 Torr; 20 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
参考文献
AMBRX, INC.
Patent: WO2007/70659 A2, 2007 ;
Location in patent: Page/Page column 172; 13/40 ;
反应条件
oxygen; copper(l) chloride in acetonitrile
T=30°C; P=760 Torr; 20 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
