N,N-二甲基苯甲酰胺合成路线 （共 319 条）
反应条件
triethylamine in diethyl ether; N,N-dimethyl-formamide; acetonitrile 1 h; Heating;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 1702 - 1708
参考文献
Popp, Frank D.; Duarte, Frederick F.; Uff, Barrie C.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1353 - 1355
反应条件
in acetonitrile T=20°C; 4 h; Irradiation; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2353 - 2360
反应条件
in tetrahydrofuran T=40 - 50°C; 3 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 7 p. 2470 - 2483
反应条件
in diethyl ether 1 h; Heating;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 326, # 4 p. 657 - 666
反应条件
bromine in tetrahydrofuran LiNMe2/complex=1.5 (Ar, -78°C, 1 h), then addn. of Br2; not isolated, detd. by gas chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C37 - C40
反应条件
ammonia; potassium; iron(II) sulfate T=-35°C; 20 h;
参考文献
Chauffaille, Jean; Hebert, Eric; Welvart, Zoltan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1645 - 1648
反应条件
ammonia; potassium; iron(II) sulfate T=-35°C; 1 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1645 - 1648
反应条件
1: H2O; methanol / 4 h / Ambient temperature 2: 75 percent / 50percent aq. NaOH, benzyltriethylammonium chloride, O2 / dimethylsulfoxide / 3 h View Scheme
参考文献
Synthesis, , # 2 p. 109 - 110
反应条件
in tetrahydrofuran LiNMe2/complex=1.5 (Ar, room temp., 2 h), then addn. of (MeO)2SO2, stirring (30 min, 25°C); not isolated, detd. by gas chromy.;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C37 - C40
