N,N-二甲基苯甲酰胺合成路线 (共 319 条)
反应条件
bis(di-tert-butylphosphinous acid)PdCl2 in acetonitrile T=25°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
tert.-butylhydroperoxide in acetonitrile T=80°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
tert.-butylhydroperoxide; sodium carbonate in acetonitrile T=20 - 60°C; 6 h; Inert atmosphereGreen chemistry;
参考文献
Saberi, Dariush; Heydari, Akbar
Applied Organometallic Chemistry, 2014 , vol. 28, # 2 p. 101 - 108
反应条件
2,2,2-trichloroethanimidamide in tetrahydrofuran T=40 - 50°C; 3 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 7 p. 2470 - 2483
反应条件
bis(tri-tert-butylphosphine)palladium(0) in toluene T=100°C; 5 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359
反应条件
N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Schroeder, Nils; Wencel-Delord, Joanna; Glorius, Frank
Journal of the American Chemical Society, 2012 , vol. 134, # 20 p. 8298 - 8301
反应条件
PdCl2(PMePh2)2 in neat (no solvent) T=100°C; P=7600 Torr; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 107, # 11 p. 3235 - 3245
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=100°C; 14 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359
反应条件
potassium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate in N,N-dimethyl-formamide T=80°C; Arylation; Elimination; 2 h;
参考文献
Olofsson; Larhed; Hallberg
Journal of Organic Chemistry, 2000 , vol. 65, # 21 p. 7235 - 7239