3-氯-4’-羟基二苯甲酮合成路线 （共 12 条）
反应条件
tri-tert-butyl phosphine; potassium carbonate; acetone; [Rh(C2H4)2Cl]2 in 1,4-dioxane; toluene
T=20 - 80°C;
参考文献
Mora, Guilhem; Darses, Sylvain; Genet, Jean-Pierre
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1180 - 1184
反应条件
aluminium trichloride
T=120 - 140°C; 0.25 h;
参考文献
Sudha; Shashikanth; Khanum, Shaukath Ara
Heterocyclic Communications, 2004 , vol. 10, # 1 p. 85 - 88
反应条件
Nafion-H in nitrobenzene
12 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Olah, George A.; Arvanaghi, Massoud; Krishnamurthy, V. V.
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3359 - 3360
反应条件
1: SOCl2 / toluene / 4 h / Heating
2: 1.) AlCl3, 2.) 1N aq. NaOH / 1.) CS2, reflux, 6 h, 2.) CS2
View Scheme
参考文献
Saiz, Enrique; Alvarez, Cristina; Riande, Evaristo; Pinto, Mauricio R.; Salom, Catalina
Journal of Chemical Physics, 1996 , vol. 105, # 18 p. 8266 - 8273
反应条件
1.1: AlCl3 / 1,2-dichloro-ethane
1.2: 1,2-dichloro-ethane
View Scheme
参考文献
Boeger, Manfred; Duerr, Dieter; Gsell, Laurenz; Hall, Roger G.; Karrer, Friedrich; Kristiansen, Odd; Maienfisch, Peter; Pascual, Alfons; Rindlisbacher, Alfred
Pest Management Science, 2001 , vol. 57, # 2 p. 191 - 202
反应条件
1.1: AlCl3 / 1,2-dichloro-ethane
1.2: 1,2-dichloro-ethane
View Scheme
参考文献
Boeger, Manfred; Duerr, Dieter; Gsell, Laurenz; Hall, Roger G.; Karrer, Friedrich; Kristiansen, Odd; Maienfisch, Peter; Pascual, Alfons; Rindlisbacher, Alfred
Pest Management Science, 2001 , vol. 57, # 2 p. 191 - 202
反应条件
sodium hydroxide; aluminium trichloride
1.) CS2, reflux, 6 h, 2.) CS2; Yield given. Multistep reaction;
参考文献
Saiz, Enrique; Alvarez, Cristina; Riande, Evaristo; Pinto, Mauricio R.; Salom, Catalina
Journal of Chemical Physics, 1996 , vol. 105, # 18 p. 8266 - 8273
参考文献
Zincke; Siebert
Chemische Berichte, 1906 , vol. 39, p. 1930
参考文献
Nakazawa; Baba
Yakugaku Zasshi, 1955 , vol. 75, p. 378,380
Chem.Abstr., 1956 , p. 2510
反应条件
aluminium trichloride
参考文献
Labor. Fournier
Patent: FR2300552DE2605382 , 19761976 ;
Chem.Abstr., 1976 , vol. 85, # 192382
